GB/T 5009.99-2003 Analytical methods for hygienic standards of polycarbonate resins for food containers and packaging materials

This standard specifies the analytical method for the sanitary standard of polycarbonate resin for food packaging. This standard is applicable to the determination of sanitary indexes of bisphenol A polycarbonate resin polymerized by melt polymerization. GB/T 5009.99-2003 Analytical method for sanitary standard of polycarbonate resin for food containers and packaging materials GB/T5009.99-2003 Standard download decompression password: www.bzxz.net

ICS 67.040
National Standard of the People's Republic of China
GB/T5009.99—2003
Representative G/18118-191
Meihol for analysis of hygienic standard ofpolycarbonate resin used as food containers andpackagingmalerials
Promulgated on August 11, 2003
Ministry of Health of the People's Republic of China
National Standardization Administration of China
Implemented on January 1, 2004
GB/T5009.99—2003
This standard replaces GB/[3]18-91 "Analysis method for hygienic standard of polycarbonate resin used as food containers andpackagingmalerials". The main adjustments of this standard and Gn/18118-01 are as follows: According to the preparation rules of G3/T20001.420018 standard Part 1, the chemical analysis method has a different structure from the standard. This standard was proposed and approved by the Health Ministry of the People's Republic of China. The standard was drafted by Shanghai Food Hygiene Inspection Institute. The main contributors to the standard are: 1 Standard
Analysis method for hygienic standard of polycarbonate resin used for food containers and packaging materials
This standard specifies the flammable resin sanitary standard for food packaging materials. This standard uses the culture method to measure the alkali-free acid of the table top. The standard is as follows: ? Normative reference documents
GBT 5009.99—2003
The following documents have become the case payments of this game through the use of this standard: A is the document of the previous month, and all subsequent payment receipts (excluding discounts and losses) will not be affected: This standard proves that the parties have reached an agreement on whether the payment volume can be used based on this standard. This is not a month-long use. The new version applies to this standard: GBT309.58 Analytical method for quick-acting polyols in food packaging G/T5009.602 CC3 Analytical method for ethyl acetate in food packaging GB/500,6-2C3
Food packaging internal ring more aldehydes hygienic standard 3 Samples
3.1 Sampling method
Use H/T9,33-2n Chinese calligraphy for sampling. 3.2 Sample sensory inspection
Take ICB samples and place them on colored paper in a single layer for sensory inspection. 3.3 Sample treatment
3.3.1 Sample conditions: weigh the sample, weigh 0.1 L of 0.3% C12 suspension: 3.3.2 Water extraction: heat the water bath at reflux for 1 h, 3.3.31 Acid extraction: heat the water bath at reflux for 6 h. 3.3.4 Alcohol extraction: heat the water bath at reflux for 1 h, 3.3.3.5 Alcohol extraction: heat the water bath at reflux for 1 h, 3.3.6 Alcohol extraction: heat the water bath at reflux for 6 h. 4.1 Extracts 4.1.1 Principle The sample is extracted by various filters: the sample is exposed to water, acid, oil and food. 4.1.2 Reagents 4.1.2.1x: distilled water or deionized water. 4.1.2.2 1% acetic acid (volume fraction). 4.1.2.3 n-dioxane, 4.1.2.4 207. ethanol (water for washing). 4.1.2.5 65% ethanol (volume fraction). 4.1.3 Collector 4.1.3.25 1lIr.T. Full gelatin system. Fe3www.bzxz.net
GB/T5009.99—2003
4.1.3.2 Water-soluble:
4.1.4 Special determination
Filter the solution after 1 day of decomposition with qualitative saturated paper, wash with the same kind of wave to a certain density, transfer to a constant amount of Fe3 solution, cool in a water bath at 15°C, weigh, and then dry in a refrigerator at 15°C. Take out the solution and put it in a cold place for 3 hours. At the same time, do a short test. 4. 1.5 Calculate the content of the compound in mg by X=(m/m)x10g. The mass of the extracted sample is in g (). The mass of the empty sample is in g (). 4.2 Consumption of manganese dioxide After water extraction, the test sample shall be processed according to Chapter 1 of GB/T533.60-203. 4.3 Gold (in Ph) After acid extraction, the test piece shall be processed according to GB/T533.50-2003. 4.4 Acid-free sample shall be processed according to GB/T533.17.1 of 221.
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