GB/T 8151.13-2000 Chemical analysis methods for zinc concentrates - Determination of germanium content

This standard specifies the method for determining the germanium content in zinc concentrate. This standard is applicable to the determination of germanium content in zinc concentrate, with a determination range of 0.00050% to 0.10%. GB/T 8151.13-2000 Chemical analysis method for zinc concentrate Determination of germanium content GB/T8151.13-2000 Standard download decompression password: www.bzxz.net

IL's73.060
National Standard of the People's Republic of China
GB/T 8151 13—200QwwW.bzxz.Net
Chemical analysis methods of zinc concentrates
Determination of germanium content
Methods for chemical analysis of zinc concentratesPeterrnination uf germanium tontcnt2000-02-16Promulgated
Implementation on 2000-08-01
Promulgated by National Quality and Technical Supervision
G/1151.13—2053
This standard adopts two workpiece analysis methods to determine the content of zinc concentrate: Method 1: Determination of the content of zinc concentrate by atomic fluorescence spectrometry\as the test method, and Method 3: Extraction and analysis by spectrophotometry of the base.
This standard complies with:
(I1S/11.1-193 Standardization work guide, unit _ standardization and expression, part 1: standardization provisions
11,4-19R standardization work, chemical analysis method, international standard T146?1978 cold metal product chemical analysis method, general provisions of the standard G/122-1087 cold metal product chemical analysis spectrophotometric method, GB/T17433998 residual product chemical analysis The basic terminology standard for chemical analysis was issued by the National Nonferrous Metals Industry Development Institute. The standard is recommended by the National Institute of Standards and Metrology of China Nonferrous Metals Industry. This standard was drafted by Ludao Zinc II. The main drafters of Method 3 of this standard are: Wang Xuan, Feng Zhiwei, and the main drafters of Method 2 are: Wang Chengzai, Li Yi 1 Scope
National Standard of the People's Republic of China
Chemical Analysis Method of Zinc Concentrate
Determination of Germanium Content
Meiludsfur Chemistry of zinc oxides and their determination by atomic fluorescence spectrometry. This standard is used for the determination of zinc content in zinc concentrates. The determination range is 0.00050--3%. 2 Method Summary
The sample is dissolved in oxygen and nitric acid. 2% acetic acid is added to sulfuric acid medium. In the presence of hydride, the zinc is reduced by potassium hydride to form chromium. The chromium is introduced into a quartz atomizer with a gas phase and the intensity of the light is measured on an optical spectrometer. 3 Reagents
3. 1 Nitric acid (1. 42 g/a).
= 0.2% pyrolytic acid.
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