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DIN EN 196-2

水泥试验方法 第2部分:水泥的化学分析

DIN EN 196-2

Methods of testing cement - Chemical analysis of cement

版本年份 1994 文件语言 英语 全文 6 页 格式 PDF
DIN EN 196-2 水泥试验方法 第2部分:水泥的化学分析封面

标准信息

STANDARD INFORMATION
标准编号
DIN EN 196-2
所属分类
DIN 德国标准
发布机构
CEN
版本年份
1994
文件语言
英语
文件格式
PDF
文件页数
6 页
文件大小
1.08 MB

中文名称为参考译名,文件语言以原文为准。

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标准简介

OVERVIEW

中文简介

该标准规定了水泥及其组成材料(如熟料和矿渣)化学分析的参考程序和替代方法。它详细描述了测定烧失量、硫酸盐、不溶残渣、硫化物、锰以及主要成分(如二氧化硅、氧化铁、氧化铝、氧化钙、氧化镁)的具体步骤。

English summary

This standard specifies the reference and alternative procedures for the chemical analysis of cement and its constituent materials, such as clinker and blastfurnace slag. It details methods for determining loss on ignition, sulfate, insoluble residues, sulfide, manganese, and main constituents including silica, iron oxide, aluminium oxide, calcium oxide, and magnesium oxide.

以上为根据文件整理的内容简介。

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4 Reagents

4.0 General requirements

Use only reagents of analytical quality and distilled water, or water of equal purity, during the analysis.

Unless otherwise stated % means % by mass.

The concentrated liquid reagents used in this standard have the following densities (ρ) (in g/cm3 at 20 °C):

hydrochloric acid1,18 to 1,19
hydrofluoric acid1,13
nitric acid1,40 to 1,42
sulfuric acid1,84
phosphoric acid1,71 to 1,75
acetic acid1,05 to 1,06
ammonium hydroxide0,88 to 0,91
triethanolamine1,12

The degree of dilution is always given as a volumetric sum, for example: hydrochloric acid 1 + 2 means that 1 volume of concentrated hydrochloric acid is to be mixed with 2 volumes of water.

4.1 Concentrated hydrochloric acid (HCl).

4.2 Dilute hydrochloric acid 1 + 1.

4.3 Dilute hydrochloric acid 1 + 2.

4.4 Dilute hydrochloric acid 1 + 3.

4.5 Dilute hydrochloric acid 1 + 9.

4.6 Dilute hydrochloric acid 1 + 11.

4.7 Dilute hydrochloric acid 1 + 19.

4.8 Dilute hydrochloric acid 1 + 99.

4.9 Dilute hydrochloric acid of pH 1,60. Add five or six drops of concentrated hydrochloric acid to 2 l water. Control the pH value by means of a pH-meter. Store the solution in a polyethylene flask.

4.10 Concentrated hydrofluoric acid (HF).

4.11 Dilute hydrofluoric acid 1 + 3.

4.12 Nitric acid (HNO3).

4.13 Concentrated sulfuric acid (H2SO4).

4.14 Dilute sulfuric acid 1 + 1.

4.15 Phosphoric acid (H3PO4).

4.16 Boric acid (H3BO3).

4.17 Acetic acid (CH3COOH).

4.18 Amino-acetic acid (NH2CH2COOH).

4.19 Metallic chromium in powder form (Cr).

4.20 Concentrated ammonium hydroxide (NH4OH).

4.21 Dilute ammonium hydroxide 1 + 1.

4.22 Dilute ammonium hydroxide 1 + 10.

4.23 Dilute ammonium hydroxide 1 + 16.

4.24 Sodium hydroxide (NaOH).

4.25 Sodium hydroxide solution 4 mol/l. Dissolve 160 g of sodium hydroxide in water and make up to 1000 ml. Store in a polyethylene flask.

4.26 Sodium hydroxide solution 2 mol/l. Dissolve 80 g of sodium hydroxide in water and make up to 1000 ml. Store in a polyethylene flask.

4.27 Ammonium chloride (NH4Cl).

4.28 Tin (II) chloride (SnCl2.2H2O).

4.29 Potassium periodate (KIO4).

4.30 Sodium peroxide in powder form (Na2O2).

4.31 Mixture of sodium carbonate and sodium chloride. Mix 7 g of sodium carbonate (anhydrous Na2CO3) with 1 g sodium chloride (NaCl).

4.32 Barium chloride solution. Dissolve 120 g of barium chloride (BaCl2.2H2O) in water and make up to 1000 ml.

4.33 Silver nitrate solution. Dissolve 5 g of silver nitrate (AgNO3) in water, add 10 ml of concentrated nitric acid (HNO3) and make up to 1000 ml with water.

4.34 Sodium carbonate solution. Dissolve 50 g of sodium carbonate (anhydrous Na2CO3) in water and make up to 1000 ml.

4.35 Potassium hydroxide solution. Dissolve 250 g of potassium hydroxide (KOH) in water and make up to 1000 ml.

4.36 Ammoniacal zinc sulfate solution. Dissolve 50 g of zinc sulfate (ZnSO4.7H2O) in 150 ml water and add 350 ml of concentrated ammonium hydroxide (NH4OH). Leave to stand for at least 24 h and filter.

4.37 Lead acetate solution. Dissolve approximately 0,2 g of lead acetate Pb(CH3COO)2.3H2O in water and make up to 100 ml.

4.38 Starch solution. To 1 g of starch (water soluble), add 1 g of potassium iodide (KI), dissolve in water and make up to 100 ml.

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